Solvent-free synthesis of (poly)thiacalix[n]arenes: The evaluation of possible mechanism based on semi-preparative HPLC separation and mass-spectrometric investigation of the reaction products
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Date
20172017
Author
Kovalev, I.S.
Rahman, M.
Sadieva, L.K.
Pavlyuk, D.E.
Giri, K.
Santra, S.
Kopchuk, D.S.
Zyryanov, G.V.
Majee, A.
Chupakhin, O.N.
Charushin, V.N.
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The interaction between p-tert-butylphenol and elemental sulfur (S8) in alkaline condition in absence of solvent at 150-170 ?C have been studied. (Poly)thiacalix[n]arenes with the phenol units connected by bi- and trisulfide bridges have been detected and characterized based on the MS data. (Figure Presented). ?ARKAT USA, Inc.
Journal
Arkivoc